Thermophysical Properties Research Laboratory, Inc.
3080 Kent Ave..
West Lafayette, In. 47906
voice: (765) 463 - 1581
fax : (765) 463-5235

Electrical Resistivity using Multiproperty Apparatus

For the central portion of an infinitely long thin rod at steady state,
and Equation 4 becomes,

where T is the uniform central temperature. By measuring V, I, and T and sample geometry, the electrical resistivity can be calculated from the relation

In Eq. (6), A is the sample cross-sectional area, L is the distance between the voltage probes, V is the voltage drop across the probes, and I is the current. The total hemispherical emittance is calculated using the same input plus the sample circumference. Equation (5) reduces to

In practice the sample diameter (and bulk density) are determined. Then voltage probes are attached over a central portion of the sample. The electrical resistivity at room temperature, the effective voltage probe separation distance, and the appropriate factors (A/L and PL_) are determined prior to insertion of the sample into the multiproperty apparatus. This is done with the aid of a knife blade holder which holds two knife blades a precisely known distance apart. The sample is connected to a regulated DC power supply in series with a reversing switch and a precision shunt. The voltage drop across the shunt, the voltage probes, and the knife blades are measured when the knife blades are located over the same general region of the sample as the voltage probes. The current flow is reversed and the procedure repeated. The measured voltage drops are averaged to eliminate stray emf effects. The current is determined from the voltage drop across the standard shunt. The resistivity is determined from Eq. (6) and the effective distance between the voltage probe wires is calculated from the relation:

The computer program RESIST collects the data and averages the measured voltages and outputs A, L, A/L, PLsigma, and rho. The system is evacuated, and the sample heated to a temperature above or equal to the highest test temperature desired. After appropriate aging, the voltage drop, current flow, and temperature are measured, the current flow reversed and the process repeated. The sample temperature is lowered to a new level and measurements repeated. This procedure is followed until the desired temperature range has been covered.


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